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AMBIENTUM BIOETHICA BIOLOGIA CHEMIA DIGITALIA DRAMATICA EDUCATIO ARTIS GYMNAST. ENGINEERING EPHEMERIDES EUROPAEA GEOGRAPHIA GEOLOGIA HISTORIA HISTORIA ARTIUM INFORMATICA IURISPRUDENTIA MATHEMATICA MUSICA NEGOTIA OECONOMICA PHILOLOGIA PHILOSOPHIA PHYSICA POLITICA PSYCHOLOGIA-PAEDAGOGIA SOCIOLOGIA THEOLOGIA CATHOLICA THEOLOGIA CATHOLICA LATIN THEOLOGIA GR.-CATH. VARAD THEOLOGIA ORTHODOXA THEOLOGIA REF. TRANSYLVAN
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Rezumat articol ediţie STUDIA UNIVERSITATIS BABEŞ-BOLYAI În partea de jos este prezentat rezumatul articolului selectat. Pentru revenire la cuprinsul ediţiei din care face parte acest articol, se accesează linkul din titlu. Pentru vizualizarea tuturor articolelor din arhivă la care este autor/coautor unul din autorii de mai jos, se accesează linkul din numele autorului. |
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STUDIA CHEMIA - Ediţia nr.2, Tom I din 2019 | |||||||
Articol: |
CONTINUOUS-FLOW ENZYMATIC KINETIC RESOLUTION MEDIATED BY A LIPASE NANOBIOCONJUGATE. Autori: MĂDĂLINA ELENA MOISĂ, LÁSZLÓ CSABA BENCZE, CSABA PAIZS, MONICA IOANA TOŞA. |
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Rezumat: This study describes the development of a continuous-flow procedure for the enzymatic kinetic resolution of rac-1-phenylethan-1-ol with the clickable acylating agent 2,2,2-trifluoroethyl 2-(prop-2-yn-1-yl-oxy)acetate, which allows facile click reaction-based downstream, enabling the large-scale chemo-enzymatic synthesis of both secondary alcohol stereoisomers with high enantiopurity. The influence of flow rate, acylating agent and substrate concentration upon the productivity of the packed-bed reactor was investigated. In addition to this, the performances of continuous-flow and batch reactors were compared. Keywords: enzymatic kinetic resolution, secondary alcohol, lipase, continuous-flow process, batch process, productivity |
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