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    STUDIA CHEMIA - Issue no. 3 / 2010  
         
  Article:   INORGANIC RINGS: EIGHT-MEMBERED Pd4S4 RING IN [Pd4Cl4{1-S-2-SCH2COOMe-C6H4-κ2S,S’}4] .

Authors:  IOANA GEORGETA GROSU, SANTIAGO GOMÉZ-RUIZ, LUMINIŢA SILAGHI-DUMITRESCU, EVAMARIE HEY-HAWKINS. 		 
       
         
  Abstract:  

Under solvothermal conditions in methanol the mononuclear complex cis-rac-[PdCl2{1,2-(HOOCCH2S)2C6H4-ĸ2S,S’}] (2) reacted to give the tetranuclear palladium(II) complex [Pd4Cl4{1-S-2-SCH2COOMe-C6H4-κ2S,S’}4] (3). The molecular structure of 3 was investigated by single-crystal X-ray structure analysis.

Keywords: palladium(II) complex, solvothermal, S-dealkylation, X-ray crystallography, inorganic ring

 
         
     
         
         
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